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6-{[(1S)-1-phenylethyl]amino}-3-(propan-2-yl)-1,2,3,4- tetrahydropyrimidine-2,4-dione

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  • 6-{[(1S)-1-phenylethyl]amino}-3-(propan-2-yl)-1,2,3,4- tetrahydropyrimidine-2,4-dione
  • 1642288-47-8
  • 273.335
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Quality Factory Supply Top Purity 99% 1642288-47-8 Customized Supply

  • Molecular Formula:C15H19N3O2
  • Molecular Weight:273.335
  • Density:1.19±0.1 g/cm3(Predicted) 

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1642288-47-8 Process route

6-chloro-3-isopropylpyrimidine-2,4(1H,3H)-dione

6-chloro-3-isopropylpyrimidine-2,4(1H,3H)-dione

(<i>S</i>)-1-phenyl-ethylamine
2627-86-3

(S)-1-phenyl-ethylamine

6-{[(1S)-1-phenylethyl]amino}-3-(propan-2-yl)-1,2,3,4- tetrahydropyrimidine-2,4-dione
1642288-47-8

6-{[(1S)-1-phenylethyl]amino}-3-(propan-2-yl)-1,2,3,4- tetrahydropyrimidine-2,4-dione

Conditions
Conditions Yield
In 1,4-dioxane; at 90 ℃;
69%
In 1,4-dioxane; for 24h;
69%
at 100 ℃; for 5h; Temperature; Inert atmosphere;
53%
1-isopropylpyrimidine-2,4,6(1H,3H,5H)trione
69998-14-7

1-isopropylpyrimidine-2,4,6(1H,3H,5H)trione

6-{[(1S)-1-phenylethyl]amino}-3-(propan-2-yl)-1,2,3,4- tetrahydropyrimidine-2,4-dione
1642288-47-8

6-{[(1S)-1-phenylethyl]amino}-3-(propan-2-yl)-1,2,3,4- tetrahydropyrimidine-2,4-dione

Conditions
Conditions Yield
Multi-step reaction with 2 steps
1: N-benzyl-N,N,N-triethylammonium chloride; trichlorophosphate / 50 °C / Inert atmosphere
2: 1,4-dioxane / 90 °C
With N-benzyl-N,N,N-triethylammonium chloride; trichlorophosphate; In 1,4-dioxane;
 

1642288-47-8 Upstream products

  • 2627-86-3
    2627-86-3

    (S)-1-phenyl-ethylamine

  • 69998-14-7
    69998-14-7

    1-isopropylpyrimidine-2,4,6(1H,3H,5H)trione

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